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B1. Sampling Process Design 45
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Page | 2/13 | Date | 14.11.2017 | Size | 14.15 Mb. | | #34041 |
| B1.1. Purpose/Background 45 B1.2.1. River Basins 46 B1.2.2. Ecoregions 46 B1.3. Indicator Variables 46 B1.4. Long-Term Design Strategy 47 B1.5. Site Selection Criteria 48 B1.6. Current Design Approach 48 B1.7. Detailed Project-Specific Sampling Plans 50 B2.1. Field Safety 52 B2.2. Available Field Equipment 53 B2.3. Bottle Types, Preservation Techniques and Holding Times 54 B2.5. Field Documentation 55 B2.6. Decontamination Procedures 55 B2.7.1. Sample Collection/Laboratory Analyses 56 B3. Sample Handling and Custody Requirements 57 B3.1. Sample Processing 57 B3.2. Sample Custody Procedure 58 B4. Analytical Methods 59 B4.1. Laboratory SOPs 59 B4.2. Analytical Units, Methods, and Holding Times 59 B4.4. Laboratory Turnaround Time Requirements 60 B4.5. Laboratory Data Report 60 B4.6. Safety and Hazardous Material Disposal Requirements 61 B4.7. Method Validation 61 B4.8. Corrective Action Process for Analytical System Failure 61 B5. Quality Control 61 B5.1. Modeling Quality Control 61 B5.2. Field Quality Control 62 B5.3. Lab Quality Control 63 B6. Instrument/ Equipment Testing, Inspection and Maintenance 63 B6.1. Computer Maintenance 63 B6.2. Purpose/ Background/Measurement Traceability 63 B6.3. Testing, Inspection, and Maintenance 66 B7.1. Model Calibration 66 B7.2. Field Instrument Calibration 67 B8. Inspection of Supplies 67 B9. Non-Direct Measurements 69 B10. Data Management 70 B10.1. GAEPD Databases 70 B10.2. Field and Lab Data Entry 71 C. ASSESSMENT AND OVERSIGHT 72 C1. Assessments and Response Actions 72 C1.1 Modeling Response Actions 74 C1.2. Organizational Assessments 75 C1.3. Assessment of Project Activities 76 C1.4. Assessment Personnel 76 D. Data Validation and Usability 78 D1. Data Review, Verification, and Validation 78 D1.1. Guidance Documents 78 D1.2. Sample Collection Procedures 78 D1.3. Sample Handling 79 D1.5. Quality Control 79 D2. Validation and Verification Methods 79 D2.1. Model Data Verification 79 D2.2. Chemical Data Verification 80 D2.3. Process for Validating and Verifying Data 80 D2.4. Biological Data Verification 80 D2.5. Process for Resolving Issues 80 D3. Reconciliation with Data Quality Objectives 81 D3.1. Reconciliation of Project Results with Data Quality Objectives 81 D3.1.1. Chemical and Bacteriological Data Reconciliation 81 D3.1.2. Biological Data Reconciliation 82 D3.1.3. Field Data Reconciliation 82 D3.2. How Data Limitation Will Be Reported 82 D3.3. Data Rejection 82
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